Differential Scanning Calorimetry

In this updated and fully revised second edition, the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important methods and aspects of Differential Scanning Calorimetry (DSC), including a sound presentation of the theoretical basis of DSC thermal analysis and temperature-modulated DSC (TMDCS). Emphasis is placed on modern evaluation techniques, instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information enables the research scientist, the analyst and experienced laboratory staff to choose the most suitable equipment, to apply DSC methods successfully, to interpret the measurement curve, and thus to measure key properties precisely. In addition, the new edition includes improved instrumental techniques such as Tzero tm and StepScan tm , new evaluation techniques, more applications, and the latest references.

Resolves the need for a practise-oriented guide to differential scanning calorimetry (DSC), the most frequently used technique in thermal analysis The authors describe the most important DSC measuring systems and programs and provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into theory and application of DSC methods The second edition has been updated and expanded; it now also includes TMDSC measurements Includes supplementary material: sn.pub/extras

Inhalt
1 Introduction.- 2 Types of Differential Scanning Calorimeters and Modes of Operation.- 3 Theoretical Fundamentals of Differential Scanning Calorimeters.- 4 Calibration of Differential Scanning Calorimeters.- 5 DSC Curves and Further Evaluation.- 6 Applications of Differential Scanning Calorimetry.- 7 Evaluation of the Performance of a Differential Scanning Calorimeter.- Appendix 1.- Appendix 2.- References.

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